Microwave-Assisted Transition Metal Nanostructure Synthesis: Power-Law Signature Verification
نویسندگان
چکیده
A power-law (y = cxn) signature between process energy budget (kJ) and density (kJ·ml-1) of microwave-assisted synthesis silver gold nanostructures has been recently described [Law Denis. AJAC, 14(4), 149-174, (2023)]. This study explores this relation further for palladium, platinum, zinc oxide nanostructures. Parametric cluster analysis statistical is used to test the over four orders magnitude as a function six microwave applicator-types metal precursor, non-Green Chemistry claimed Green Chemistry. It found that Chemistry, ranges from 0.291 900 kJ, with residual error ranging −33 +25.9 kJ·ml-1. The higher range 3.2 kJ 3.3 MJ, −33.3 +245.3 also profile time produced by software controlled digestion applicators poorly reported which leads problematic outliers produce possible phase-transition in signature. original Au Ag database new Pd, Pt ZnO (with without outliers) yield global constants c 0.7172 ± 0.3214 kJ·ml-1 at x-axes 0.001 exponent, n 0.791 0.055. information aimed understand variations historical processes, develop scale-out through intensification.
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ژورنال
عنوان ژورنال: American Journal of Analytical Chemistry
سال: 2023
ISSN: ['2156-8278', '2156-8251']
DOI: https://doi.org/10.4236/ajac.2023.148018